- Introduction to powder XRD
- Applying PXRD analysis in the pharmaceutical industry
- Theory of XRD
- Data viewer scan image
- Overlays, file conversion utility
- Basic data processing using Highscore software
- Background, Peak search algorithm
- Profile fitting, FWHM, clip range, smoothing, Peak Labelling
- Batch and report creation etc
- Basic & advanced optical modules like Bragg BrentanoHD
- Sample stages and detectors
- Basic approach to polymorphism and amorphous quantification
- High throughput screening and cluster analysis
- Effects of preferred orientation
- How to minimise sample preparation errors: front loading vs backloading examples
- Managing low volume samples
- Transmission holders (including capillary)
- Polymorphic screening and pattern simulation
- Crystallinity and amorphous quantification
- Importance of particle size analysis to check on API bioavailability, efficacy etc
- *New* Mastersizer 3000+ for particle size distribution analysis
- Data collection strategies
- Method development and the importance of scan range, step size, time per step, AL, scan models, fast scan/slow scan
- Challenges and how to overcome them for achieving the best LODs, LOQs
- Signal to noise ratio
- Cluster analysis
- Bitmap conversion
2-days Advanced Pharma XRD OTP: Vadodara
25 - 26 April | 9:00-17:00 India Time | Fortune Inn Promenade Vadodara
About The Event
2-days “FREE ADVANCED OPERATOR TRAINING PROGRAM”, Exclusively for XRD Users in Pharma Industry Who should attend? • Sr. Operators or New XRD Operators in Pharma Industry (0-15 years exp.) • Users of XRD for Pharma • R&D or QC Heads • Managers What will you learn? • PXRD fundamentals • Critical sample preparation practices • Proper experimental set up • Improving data quality with good sample preparation • Data analysis & interpretation • Advanced data analysis on polymorphism, crystallinity, S/N & amorphous quantification, cluster analysis, Bitmap conversion and more
More Information
HURRY – LIMITED SEATS AVAILABLE!
Day 1: |
Day 2: |
Overview |
Recap and Q & A XRD data processing |
Tea break |
Tea break |
Optimising your XRD experimental set up for superior data quality |
Introduction to XRD applications |
Lunch break |
Lunch break |
Importance of good sample preparation for superior results |
Advanced XRD data processing Complementary analytical methods |
Tea break |
Tea break |
Introduction to data collection |
HighScore demonstration |
Q & A / End |
Q & A / End |